Synthesis and Formulation of Polymer Materials

7L Instrumented batch reactor (pilot plant) for polycondensation

1L batch reactor for Ziegler-Natta synthesis

Supercritical CO2 Reactor 100mL

Instrumented High Viscosity continuous medium - twin screw extrudors (x 3)

Temperature-controlled 20 L reactor formulation

20L solid state polymerization reactor
Methods of Preparation and Forming of Polymer Materials

Instrumented co-rotating twin screw extruders (screw profiles designable) (x3) : CLEXTRAL (2)

Single screw extruders nstrumented (x7) : CAMIL, Thorette, FAIREX, KAUFFMAN

Slide-screw extruding Visio (Oyonnax INSA site)

DSM twin-screw micro-extruder (max 15g) Equipped With injection machine and film / fiber processing

Film cast dies and processing (x2) (thickness from 50 to 500 m)

Instrumented mixers (x3) : Rheocord HERAEUS, Haake (2)

Reaction Injection Molding RIM

Resin Transfer Molding RTM

Calanders (x2)

Lab-scale film blowing Babyplast

Visio-vis (transparent Instrumented extrudor) (Oyonnax INSA site)

Instrumented rotomolding (Oyonnax INSA site)

Injection Machine (x4) (from 20 to 90T) : BILLON, Sandretto, KLOCKNER

Micro-injection machine Babyplast

Instrumented injection press (Oyonnax INSA site)

Compression presses (x4) : hot and cold courses

Thermoforming press ILLIG

Co-extrusion line (Oyonnax INSA site)

Bar-coater

Plasma Surface Treatment of

Micro-Plasma Treatment of Surface Waves

Eximer laser surface treatment

UV oven (time and spectrum controlled)

Spin coater

Langmuir-Blodgett balance

Platform Coatings / Paint CoatingXpert
Physical Characterization of Polymer Materials and Multimaterials

Size Exclusion Chromatography SEC - UV / IR / Light Scattering Detectors (x2) : WATERS

Size Exclusion Chromatography Hot temperature SEC WATERS

HPLC Chromatography - Preparative CPV Coupled With Mass Spectrometry

Inverse Gas Chromatograph

Gas Phase Chromatography Coupled With Mass Spectrometry

Calorimetry DSC analysis (x7) (TA (4), METLLER (2), Setaram), Perkin-Elmer UV DSC, modulated DSC Perkin-Elmer

Thermogravimetric Analysis - TGA, TGA - GC / MS / IR

FT-IR spectrometers MIR (x 3)

FT-NIR spectrometers ir - on-line coupling With Processes

UV Spectrometer

Malvern Particle Size Measurement

Turbidimetry measurements

Solid State Spectrometers for viscoelastic characterization

Rheometric RMS 800 / RDA2 / RSA2 and ANTON-PARR

Rheometers for molten and liquid states (reactive or not) Rheological characterization -

Rheometric RMS 800 / DDR 700 / RDA2 / ARES / ANTON-PARR

Shear Rheometers Controlled Stress (x3) : TA 3000, SR5000

Combined with optical microscopy Rheometer

Capillary Rheometers (x3) : MALVERN, INSTRON 3211 (2), HAAKE

Elongational Rheometer Rheometrics RME

MFI Measurements (x2)

Application related Rheometers : RHEOMAT (x2), Kinematics (x2), THROMBOMAT (x2), BROOKFIELD

Tensile machines (from few "grams up to 20T) (x8) Equipped With low / high temperature-controlled chambers and extensometers

Instrumented Charpy (x2) and Notched impact tests

Hydraulic tensile machine Equipped With low / high temperature-controlled chamber fatigue testing, impact tests (Charpy, multi-axial)

Heat Distortion Temperature and Vicat measurements

Electrical and spectroscopic dielectrical

Microdielectrometers (x3)

Gas and Vapor permeameters

Vapor adsorption scales

Optical microscopy (x 4) With hot METLLER internships (x3)

Atomic Force Microscope (AFM) (x2) : tapping mode, lateral force, phase contrast, temperature-controlled liquid and internships

Wilhemy scales (x3)

Ellipsometry

Surface tension measurements : sessile drop - Including Hot internship - (X4)
Simulation

Accelrys Software - Materials Studio molecular modeling : Atomistic, coarse grain, mesoscale

Parallel processing computers for simulations
Access to other platforms

CLYME - Electron Microscopy Center of Lyon

FR2151 CNRS - Platform NMR of Polymers Lyonnais

Centre for Microscopy Université Claude Bernard Lyon I

Center for X-ray diffraction characterization - University Lyon I

Quantimeter Center - University Claude Bernard Lyon I / Faculty of Pharmacy, Lyon

ESRF Beam line - Grenoble

LLB CEA Saclay Neutron Scattering